Self healing of creep damage in iron-based alloys by supersaturated tungsten

Self healing of creep damage in iron-based alloys by supersaturated tungsten

Fang, H. (TU Delft Novel Aerospace Materials; TU Delft RST/Fundamental Aspects of Materials and Energy)
Szymanski, N. (Student TU Delft)
Versteylen, C.D. (TU Delft RST/Fundamental Aspects of Materials and Energy)
Cloetens, P. (European Synchrotron Radiation Facility)
Kwakernaak, C. (TU Delft (OLD) MSE-1)
Sloof, W.G. (TU Delft (OLD) MSE-1)
Tichelaar, F.D. (TU Delft QN/Afdelingsbureau; Kavli institute of nanoscience Delft)
Balachandran, S. (Max-Planck-Institut für Eisenforschung)
Herbig, M. (Max-Planck-Institut für Eisenforschung)
Brück, E.H. (TU Delft RST/Fundamental Aspects of Materials and Energy)
van der Zwaag, S. (TU Delft Novel Aerospace Materials; Tsinghua University)
van Dijk, N.H. (TU Delft RST/Fundamental Aspects of Materials and Energy)

2019

When metals are mechanically loaded at elevated temperatures for extended periods of time, creep damage will occur in the form of cavities at grain boundaries. In the present experiments it is demonstrated that in binary iron-tungsten alloys creep damage can be self healed by selective precipitation of a W-rich phase inside these cavities. Using synchrotron X-ray nano-tomography the simultaneous evolution of creep cavitation and precipitation is visualized in 3D images with a resolution down to 30 nm. The degree of filling by precipitation is analysed for a large collection of individual creep cavities. Two clearly different types of behaviour are observed for isolated and linked cavities, where the isolated cavities can be filled completely, while the linked cavities continue to grow. The demonstrated self-healing potential of tungsten in iron-based metal alloys provides a new perspective on the role of W in high-temperature creep-resistant steels.

Creep damage
Self-healing
Steel
Synchrotron radiation
Tomography

http://resolver.tudelft.nl/uuid:4b0820a5-5fd6-4fe5-bffc-5da2ed9748e9

https://doi.org/10.1016/j.actamat.2019.01.014

2019-08-01

1359-6454

Acta Materialia, 166, 531-542

Green Open Access added to TU Delft Institutional Repository ‘You share, we take care!’ – Taverne project https://www.openaccess.nl/en/you-share-we-take-care Otherwise as indicated in the copyright section: the publisher is the copyright holder of this work and the author uses the Dutch legislation to make this work public.

Institutional Repository

journal article

© 2019 H. Fang, N. Szymanski, C.D. Versteylen, P. Cloetens, C. Kwakernaak, W.G. Sloof, F.D. Tichelaar, S. Balachandran, M. Herbig, E.H. Brück, S. van der Zwaag, N.H. van Dijk